[en] This thesis details the development, validation, and application of advanced solid-state nuclear Magnetic resonance spectroscopy (NMR) techniques for the characterization of the silica surface in raw materials and in rubber compounds. The performance of the quantitative techniques (29Si DP-CPMG, SVD and 29Si multiCP) and qualitative techniques (29Si CP-CPMG and {1H-29Si}-1H MCPi) are investigated using model and close-to-real life samples. The insights gained from this study are useful for the surface-specific characterization of silica and could offer clues for similar topics.
Disciplines :
Chemistry
Author, co-author :
Yan, Chuanyu ; University of Luxembourg > Faculty of Science, Technology and Medecine (FSTM)
Language :
English
Title :
Advanced Characterizations of Silica Surface in Rubber Compounds by Solid-State Nuclear Magnetic Resonance Spectroscopy
Defense date :
07 October 2021
Institution :
Unilu - University of Luxembourg, Esch-sur-Alzette, Luxembourg
