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See detailAdvanced Characterizations of Silica Surface in Rubber Compounds by Solid-State Nuclear Magnetic Resonance Spectroscopy
Yan, Chuanyu UL

Doctoral thesis (2021)

This thesis details the development, validation, and application of advanced solid-state nuclear Magnetic resonance spectroscopy (NMR) techniques for the characterization of the silica surface in raw ... [more ▼]

This thesis details the development, validation, and application of advanced solid-state nuclear Magnetic resonance spectroscopy (NMR) techniques for the characterization of the silica surface in raw materials and in rubber compounds. The performance of the quantitative techniques (29Si DP-CPMG, SVD and 29Si multiCP) and qualitative techniques (29Si CP-CPMG and {1H-29Si}-1H MCPi) are investigated using model and close-to-real life samples. The insights gained from this study are useful for the surface-specific characterization of silica and could offer clues for similar topics. [less ▲]

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